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×Recrystallization of Ni3Al Base Single Crystal Alloy IC6SX with Different Surface Mechanical Processes

Yanan Li Yafang Han

材料科学技术(英)

The recrystallization behavior of Ni3Al base single crystal alloy IC6SX with different mechanical processes has been studied.The specimens of the alloy were treated by surface cleaning and cold working during the blades manufacture, and then heat treated in the temperature range of 800{1260°C for 1 h to 4 h. The microstrcture of the specimens were examined by optical and scaning electron microscopy, and the room temperature tensile property, stress rupture property under the test condition of 1100°C/130 MPa, and the thermal cycle fatigue resistance under 1100−20°C of the specimens with and without recrystallization were carried out. The experimental results showed that the initial recrystallization nucleation temperatures of the alloy by dry grit blasting, wet grit blasting, indentation, shot blasting and burnishing were 900−950°C/1 h, 1000−1100°C/1 h, 1200−1220°C/4 h, 1220−1240°C/1 h and 1220−1240°C/1 h, respectively and the primal recrystallization completing temperatures of the alloy by those mechanical processes mentioned above were 1200−1210°C/1 h, 1100−1200°C/1 h, 1220−1240°C/4 h, 1240−1260°C/1 h and 1240−1260°C/1 h, respectively. The results also indicated that the deformation amount of the specimens by burnishing and dry grit blasting was bigger than that by wet grit blasting and shot blasting according to their recrystallization  emperature and the micro-hardness profile below the surface of specimens. It has been found that the recrystallization had no evident effect on mechanical properties of the alloy.

关键词: Ni3Al , single crystal alloy , recrystallization , surface layer

化学热处理改善 Ti-6Al-4V 钛合金耐空蚀性能的研究

李海斌 , 崔振铎 , 李朝阳 , 朱胜利 , 杨贤金

功能材料 doi:10.3969/j.issn.1001-9731.2014.07.031

利用渗氮、渗碳和碳氮共渗3种化学热处理方法对 Ti-6Al-4V 钛合金表面进行改性,制备出3种不同成分的硬质表面层。利用 SEM、XRD 和 Vickers显微硬度仪分别对3种表面层的微观形貌和结构、化学组成、显微硬度进行了表征,并利用磁致伸缩振动空蚀设备研究了表面层的耐空蚀性能。结果表明通过3种化学热处理均在 Ti-6Al-4V 钛合金表面形成了致密的硬质陶瓷层。该硬质陶瓷层在空蚀过程中可以抑制裂纹在表面过早的形成和向基体扩展,从而延长了空蚀的孕育期和显著地改善了钛合金的耐空蚀性能。

关键词: 钛合金 , 化学热处理 , 显微组织 , 表面层 , 耐空蚀

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